Spin Coating Simulator - Tutorial (Print Version)

πŸ”¬ SPIN COATING SIMULATOR

Complete User Tutorial

Β© 2025 KEEPLEAN Educational Tools | Toufik Dakhia LSS Master Black Belt

πŸ“– How to Use This Tutorial:
  • Print: Click the blue button (top right) β†’ Print or Save as PDF
  • Navigate: Use browser Find (Ctrl+F) to search topics
  • Practice: Follow along with the simulator open

πŸ“‹ Table of Contents

  1. Introduction
  2. Quick Start (60 seconds)
  3. Interface Overview
  4. Material Parameters
  5. Speed Profile (4 Phases)
  6. Environmental Control (PID)
  7. Running a Simulation
  8. Understanding Results
  9. Exporting Data
  10. Practical Examples

1. Introduction

What is Spin Coating?

Spin coating is a process used to apply uniform thin films to flat substrates. A solution is deposited on a substrate which is then rotated at high speed to spread the fluid by centrifugal force.

🎯 Learning Objectives:
  • Understand how process parameters affect coating thickness
  • Learn the relationship between viscosity, speed, and thickness
  • Master environmental control (PID systems)
  • Perform statistical analysis of coating uniformity
  • Apply Design of Experiments (DOE) principles

Simulator Capabilities

Feature Description
πŸ§ͺ Materials 6 different photoresists (from easy to difficult)
βš™οΈ Speed Profile 4-phase customizable process
🌑️ Environment Temperature & humidity control with PID tuning
πŸ“ Measurement 50-point uniformity analysis
πŸ“Š Statistics Average, Std Dev, CV%, Uniformity
πŸ“₯ Export CSV & Excel data export

2. Quick Start (60 Seconds)

✨ Follow these steps to run your first simulation:
Step 1: Select Material β†’ Choose AZ 1518 (beginner-friendly)
Step 2: Set Quantity β†’ Enter 100 Β΅L
Step 3: Configure Speed Profile:
  • Phase 1: 10 rpm, 2 s
  • Phase 2: 10 β†’ 500 rpm, 5 s
  • Phase 3: 2000 rpm, 15 s
  • Phase 4: 3000 rpm, 15 s
Step 4: Set Environment:
  • Temperature: 22Β°C
  • Humidity: 45%
  • Keep default PID values
Step 5: Click ▢️ START SIMULATION
Step 6: Wait 2-3 seconds for results
Expected Results:
  • Average Thickness: ~2.5 Β΅m
  • Uniformity: >95% (Green indicator)
  • CV%: <2%

4. Material Parameters

Available Materials

Material Viscosity Difficulty Typical Use Thickness @ 3000 rpm
AZ 1518 25 cP ⭐ Easy Photolithography ~1.7 ¡m
S1813 40 cP ⭐ Easy Standard resist ~2.1 ¡m
PMMA 950K 35 cP ⭐⭐ Medium E-beam lithography ~2.0 ¡m
SU-8 2050 450 cP ⭐⭐ Medium Thick films, MEMS ~7.0 ¡m
HSQ 12 cP ⭐⭐⭐ Hard Nanofabrication ~0.8 ¡m
Ma-N 2403 18 cP ⭐⭐⭐ Hard High resolution ~1.0 ¡m
⚠️ Beginner Tip: Start with AZ 1518 or S1813 for best results

Resin Quantity

Wafer Size Recommended Quantity
50mm 50-100 Β΅L
100mm 100-200 Β΅L
200mm 200-500 Β΅L
Effect on coating:
  • More resin (↑) β†’ Thicker coating
  • Less resin (↓) β†’ Thinner coating

5. Speed Profile (4 Phases)

SPEED (rpm)
    ↑
5000β”‚                              β”Œβ”€β”€β”€β”€β”€β”€β”€β”€β”€β”€β”€β”€β”€β”€β”€β”€β”€β”€β”
    β”‚                              β”‚   Phase 4        β”‚
3000β”‚                     β”Œβ”€β”€β”€β”€β”€β”€β”€β”€β”€   DRYING         β”‚
    β”‚                     β”‚        β”‚                  β”‚
2000β”‚                     β”‚ Phase 3β”‚                  β”‚
    β”‚                    β•±β”‚ THIN   β”‚                  β”‚
 500β”‚                   β•± β”‚        β”‚                  β”‚
    β”‚     β”Œβ”€β”€β”€β”€β”€β”€β”   β•±Phaseβ”‚        β”‚                  β”‚
  10│──────Phase1β”‚ β•±  2   β”‚        β”‚                  β”‚
    β”‚     β”‚SPREADβ”‚RAMP    β”‚        β”‚                  β”‚
   0└─────┴──────┴─────────┴────────┴──────────────────┴───→ TIME
         2s      5s       15s       15s
    

Phase 1: Deposit (Spreading)

Purpose: Spread the resin across the wafer
Speed: 10-50 rpm (Low speed)
Time: 2-5 seconds
⚠️ IMPORTANT: Speed must be β‰₯ 5 rpm

Phase 2: Acceleration Ramp

Purpose: Gradually increase speed to prevent splashing
From: 10-100 rpm
To: 500-2000 rpm
Time: 3-10 seconds

Phase 3: Speed Thinning

Purpose: Achieve desired thickness
Speed: 1000-4000 rpm (High speed)
Time: 10-30 seconds
Key: Film thickness is determined mainly in this phase

Phase 4: Final Drying

Purpose: Evaporate remaining solvent
Speed: 2000-5000 rpm (Very high speed)
Time: 10-30 seconds
Phase Speed Range Duration Purpose
1 - Deposit 10-50 rpm 2-5 s Spread resin
2 - Ramp 10β†’2000 rpm 3-10 s Smooth acceleration
3 - Thinning 1000-4000 rpm 10-30 s Set thickness
4 - Drying 2000-5000 rpm 10-30 s Evaporate solvent

8. Understanding Results

Statistics Overview (50 measurement points)

Statistic What It Means Good Value
Average Thickness (Β΅m) Mean thickness across all 50 points Target Β±10%
Std Dev Οƒ (Β΅m) Measure of thickness variation < 0.1 Β΅m
CV% Coefficient of Variation = (Οƒ/avg) Γ— 100 < 2%
Min (Β΅m) Thinnest point measured Check spec minimum
Max (Β΅m) Thickest point measured Check spec maximum
Uniformity (%) [1 - (Max-Min)/(2Γ—Avg)] Γ— 100 β‰₯ 95%

Uniformity Interpretation

Value Color Quality Use Case
β‰₯ 95% 🟒 Green Excellent Production ready
90-95% 🟑 Yellow Good Development acceptable
< 90% πŸ”΄ Red Poor Not acceptable
Industry Standards:
  • Production: β‰₯ 98%
  • Development: β‰₯ 95%
  • Research: β‰₯ 90%

10. Practical Examples

Example 1: Speed Effect Study

Objective: Understand how speed affects thickness
Run Phase 3 Speed Expected Thickness (AZ 1518)
1 1000 rpm ~5.0 Β΅m
2 2000 rpm ~2.5 Β΅m
3 3000 rpm ~1.7 Β΅m
4 4000 rpm ~1.3 Β΅m
Analysis: Create plot with Speed (X-axis) vs Thickness (Y-axis)
Expected: Thickness ∝ Speed-0.5 (inverse square root relationship)

Example 2: Material Comparison

Objective: Compare all 6 materials at same speed
Material Viscosity Expected Thickness @ 3000 rpm
HSQ 12 cP ~0.8 Β΅m
Ma-N 2403 18 cP ~1.0 Β΅m
AZ 1518 25 cP ~1.7 Β΅m
PMMA 35 cP ~2.0 Β΅m
S1813 40 cP ~2.1 Β΅m
SU-8 450 cP ~7.0 Β΅m
Analysis: Plot Viscosity vs Thickness
Expected: Thickness ∝ √Viscosity

Troubleshooting Guide

Common Issues & Solutions

Problem Possible Cause Solution
Error: "Phase 1 must be β‰₯ 5 rpm" Phase 1 speed too low Set Phase 1 to 10 rpm or higher
Poor Uniformity (<90%) Environmental instability Reduce Kp and Ki, add small Kd (0.05)
Poor Uniformity (<90%) Insufficient resin Increase quantity to 100 Β΅L or more
Thickness too high Speed too low / Temp too low Increase speed or temperature
Thickness too low Speed too high / Temp too high Decrease speed or temperature
Export doesn't work No simulation run yet Run simulation first, then export

Quick Reference Card

Default Settings (Beginner)

Parameter Value
Material AZ 1518
Quantity 100 Β΅L
Phase 1 10 rpm, 2 s
Phase 2 10β†’500 rpm, 5 s
Phase 3 2000 rpm, 15 s
Phase 4 3000 rpm, 15 s
Temperature 22Β°C
Humidity 45%
PID Kp=4.0, Ki=1.0, Kd=0.0

Key Formulas

Thickness Equation:
h = K Γ— √(Ξ·/ρ) / Ο‰
h: thickness, Ξ·: viscosity, ρ: density, Ο‰: angular velocity
Viscosity-Temperature:
Ξ·(T) = Ξ·β‚€ Γ— exp(-0.03 Γ— Ξ”T)
Ξ”T = T - 22Β°C
Uniformity:
U = [1 - (Max-Min)/(2Γ—Avg)] Γ— 100%
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